ICDD X-ray Diffraction Clinics

xrd clinics

Session I - Fundamentals of X-ray Powder Diffraction -  2-6 June 2014 - Register
Session II - Advanced Methods in X-ray Powder Diffraction - 9-13 June 2014
- Register

or Register for both Sessions

History of the Clinic
The ICDD X-ray Clinics are a continuation of the SUNY Clinics which were held at the State University of New York at Albany for 25 years. In 1990, the International Centre for Diffraction Data (ICDD) assumed responsibilities for these clinics. ICDD is a nonprofit, scientific organization which publishes the Powder Diffraction File™ and the journal, Powder Diffraction. ICDD is committed to promoting the applications of materials characterization methods in science and technology by providing educational programs such as the ICDD Clinics.

Purpose
During the past seven decades, the use of X-ray analytical methods has seen continued growth in the areas of materials characterization and phase identification. Over the years, the development of procedures, techniques, and advanced equipment have greatly enhanced the versatility of the method.  The purpose of the X-ray clinic is to provide participants with a fundamental understanding of the theoretical basis as well as the practical application and implementation of powder diffractometry in today’s laboratory.  This knowledge and understanding is applicable whether the attendee works in academia, industry, or government laboratory, or whether they are a student, professor, researcher, or analyst.

Scope
The clinic is presented in two separate week-long sessions, each of which stands alone as a complete course. Session I, Fundamentals of X-ray Powder Diffraction, is directed to both relative newcomers in the field and to more experienced users wishing to broaden their understanding of fundamental concepts and established procedures. The major emphases of Fundamentals of X-ray Powder Diffraction are the acquisition of reliable experimental data and qualitative phase identification using both manual and automated search techniques. Session II, Advanced Methods in X-ray Powder Diffraction, is designed for the experienced user and focuses on computer-based methods of qualitative and quantitative phase analysis, as well as crystal structure analysis and refinement. For maximum benefit from the Advanced Methods in X-ray Powder Diffraction, the ICDD Clinic staff strongly recommends that students have previously attended Session I. 

If you have questions regarding the level of experience required for Session II, please contact:

Cyrus Crowder
ICDD Headquarters
Phone: (610) 325-9814
FAX: (610) 325-9823
E-mail: crowder@icdd.com

Many attendees of the clinics have found it advantageous to attend the two sessions in successive years.

Which Clinic Should You Attend?
Use our handy Excel Quiz to determine if you should be attending Session I or Session II.

Self-help guideline for XRD knowledge/experience needed for XRD II clinic

  0 pts 1pt 2pt Your score
Experience with X-ray powder diffraction for phase identification < 1 year 1-5 years > 5 years  
Use of calibration standards No non-routine routine  
Cognizant of preferred orientation problems and particle statistics in sample No somewhat always  
Understand X-ray filters and monochromators No limited Yes  
Can name the 7 crystal systems No with hints Yes  
Understand Miller indices No kinda Yes  
Comfortable tailoring the diffractometer experiment to both the specimen and the information being sought No occasionally Yes  
Understand space group information: Hermann-Maguin symbols, Wyckoff positions, reflection conditions, symmetry elements No 2 of the 4 all 4  
Use of Rietveld refinement Never a few times frequently  
         
Obtain a sum of 12 or more (or have taken XRD I) before considering XRD II Sum=  

 

Format
The format of the clinic is a combination of morning lectures and afternoon recitations and workshops. Ample opportunity for individual student-faculty interaction exists throughout each week, including small recitation and workshop groups and a session where students can discuss their applications and problems with the entire faculty.

Course Outline
Session I - Fundamentals of X-ray Powder Diffraction - 2-6 June 2014 - Register

  • Production and properties of X-rays: continuous and characteristic radiation, absorption, scatter and diffraction
  • Production of monochromatic X-radiation: choice of source conditions, use of beta-filters, proportional detectors and pulse height selection, monochromators, use of the Si(Li) and Ge(Li) detectors
  • Constituents of the diffraction pattern: expected reflections, Miller indices, unexpected reflections, effect of scatter and fluorescence, factors affecting peak positions and intensities
  • The powder diffractometer: optical arrangement, factors affecting instrumental profile widths; choice and function of divergence slits, calibration and alignment, detectors, X-ray optics
  • Acquisition of good diffraction data: specimen requirements, preparation techniques, use of standards, and proper operation of powder diffractometers
  • Qualitative phase identification: the Powder Diffraction File™, quality of reference patterns, the Alphabetical, Hanawalt, and Fink Indexes, automated methods, and specialized subfiles
  • Industrial applications of X-ray powder diffraction
  • Hands-on use of personal computers for demonstration of the latest software
  • Data mining with the PDF

Session II - Advanced Methods in X-ray Powder Diffraction - 9-13 June 2014 - Register

  • Brief review of fundamentals
  • Factors affecting accuracy of measured 2theta values: intensity aberrations, specimen displacement, specimen transparency, diffractometer alignment, and the use of external and internal standards
  • Factors affecting intensities of diffraction peaks: structure-sensitive properties, specimen-sensitive effects, and measurement-sensitive effects
  • Use of computer methods for data reduction and qualitative phase identification: peak-hunting methods, alpha2 stripping, search/match techniques and the Powder Diffraction File™, use of elemental data, error windows and probability searching, and scoring algorithms
  • Advanced data mining with the PDF
  • Exploration of powder pattern indexing methods
  • Quantitative analysis: specimen preparation considerations, Reference Intensity Ratios, absorption correction methods, matrix-flushing methods, and whole-pattern analysis using the Rietveld method
  • Structure solution and refinement using the Rietveld method

or Register for both Sessions

Clinic Faculty
The clinic faculty is selected from academic, industrial and government institutions under the direction of ICDD Management. 
Read Faculty Bios.

Schedule
Sessions are held Monday through Wednesday from 8:30 a.m. to 4:30 p.m., Thursday from 8:30 a.m. to 6:00 p.m., and Friday from 8:30 a.m. to 12:00 p.m.

Fees & Registration
Registration fees for training courses include classroom and lab materials and catered lunches. Registrations must be received no later than six weeks prior to the start of the course. Payment must be received prior to the course to attend.
Register Online or
fax the registration form to +610-325-9823!

Fundamentals of X-ray Powder Diffraction - $1,830 USD
Advanced Methods in X-ray Powder Diffraction - $1,830 USD
Fundamentals of XRD and Advanced Methods in XRD two-week course - $3,300 USD

Tuition Waiver Opportunities

Cancellation Policy
ICDD must guarantee payment for meals and materials in advance.You will receive a 50% refund of the paid registration fee if your written cancellation is received at ICDD twenty business days prior to the start of class.With less notice, a colleague may take your place, or the course materials will be mailed to you.

Location
ICDD Headquarters
12 Campus Boulevard
Newtown Square, Pennsylvania, 19073-3273 U.S.A.
Phone: +610.325.9814

Download Registration Form - Online Registration for XRD I, XRD II, Both XRD I and II

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