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PPXRD-8 Workshop Presentations (.pdf)

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Optional Workshop
Characterization of Pharmaceutical Solids
Monday, 4 May
9.00-17.00

Workshop instructors are scientists from academia, industry and the International Centre for Diffraction Data. In order to facilitate the participation of postgraduate students and young scientists, the workshop will begin with a talk on the fundamentals of XRD, followed by an introduction to pharmaceutical materials science. The topics to be covered in the workshop are:

  • Instrumental and software advances
  • Direct analysis of pharmaceutical dosage forms
  • Quantitative phase analyses
  • Use of XRD in the characterization of nanomaterials and amorphous phases
  • Effective use of Powder Diffraction File (.pdf) (Fawcett)
  • Applications of high intensity X-radiation
  • Regulatory applications of XRD (including QbD)

Workshop Instructors:
Dr. Raj Suryanarayanan, Workshop Chair, University of Minnesota, U.S.A.
Dr. Detlef Beckers, PANalytical, The Netherlands
Dr. Cyrus Crowder, ICDD, Newtown Square, PA, U.S.A.
Dr. Tim Fawcett, ICDD, Newtown Square, PA, U.S.A.
Dr. Geert Vanhoyland, Bruker-AXS GmbH, Germany

Tuesday, 5 May - 8.30-17.20

Type Title of Paper Speaker & Affiliation
Morning Organic Crystal Structure Prediction
Session Chair: Dr. Detlef Beckers,
PANalytical, Almelo, The Netherlands
Invited COMPUTED CRYSTAL ENERGY LANDSCAPES AS AN AID TO UNDERSTANDING POLYMORPHISM (.pdf) Sarah (Sally) L. Price, University College London, London, U.K.
Contributed POWDER DIFFRACTION AND CRYSTAL STRUCTURE PREDICTION: A TWO-WAY RELATIONSHIP (.pdf) Maryjane Tremayne, University of Birmingham, Birmingham, U.K.
  XRPD Structural Techniques (Acquisition and Use of XRPD Data, Indexing, Structure Determination, Rietveld Refinement)
Session Co-chairs: Dr. Ken Shankland,
Reading University, Reading, U.K. and Dr. Arnt Kern, Bruker AXS GmbH, Karlsruhe, Germany
Invited ADVANCES IN CRYSTAL STRUCTURE SOLUTION BY EXPO2008 (.pdf) Angela Altomare, IC-CNR, Bari, Italy
Afternoon Formulation, Product Development, Drug Delivery and Polymorph & Salt Screening
Session Chair: Dr. Shawn Yin,
Bristol-Myers Squibb Company, New Brunswick, NJ, U.S.A.
Contributed MANY PATTERNS AND MANY METHODS: NEW METHODS UTILISING MULTIPLE ANALYSIS TECHNIQUES IN POLYMORPH AND SALT SCREENING SYSTEMS (.pdf) Gordon Barr, University of Glasgow, Glasgow, Scotland, U.K.
Contributed PARTICLE SIZE ANALYSIS BY TWO-DIMENSIONAL XRD (.pdf) Bob He, Bruker-AXS, Inc., Madison, WI, U.S.A.
Contributed MATERIAL IDENTIFICATION:
THE DESCRIPTIVE STATISTICS OF PHASE IDENTIFICATION
(.pdf)
Timothy Fawcett, ICDD, Newtown Square, PA, U.S.A.

Wednesday, 6 May - 8.30 – 17.35
Morning Amorphous, Activated and Nanomaterials
Session Chair: Dr. Julien Giovannini,
AstraZeneca, Nottingham, U.K. 
Type Title of Paper Speaker & Affiliation
Invited PHYSICAL STABILITY OF AMORPHOUS SOLID DISPERSIONS: XRPD AND COMPUTATIONAL STUDIES OF ‘MISCIBILITY’ (.pdf) Igor Ivanisevic, SSCI, a division of APTUIT Inc., West Lafayette, IN, U.S.A.
Invited CRYSTALLITE SIZES AND MICROSTRAINS DETERMINED BY RIETVELD REFINEMENT: APPLICATION TO MILLED LACTOSE (.pdf) Vincent Caron, Trinity College Dublin, Dublin, Ireland
Contributed CHARACTERISATION AND PREDICTION OF STABILITY OF AMORPHOUS MATERIALS DURING PHARMACEUTICAL DEVELOPMENT: PAIR-WISE DISTRIBUTION FUNCTION (.pdf) Helen Blade, AstraZeneca, Macclesfield, Cheshire, U.K.
Contributed DIFFRACTION, NON-CRYSTALLINITY, AND THE PDF DATABASE (.pdf) Cyrus Crowder, ICDD, Newtown Square, PA, U.S.A.
Contributed STUDYING AMORPHOUS PHARMACEUTICAL MATERIALS BY POWDER X-RAY DIFFRACTION AND OTHER SOLID-STATE TECHNIQUES (.pdf) Shawn Yin, Birstol-Myers Squibb, New Brunswick, NJ, U.S.A.
Contributed QUANTITATIVE ANALYSIS OF PHASES WITH PARTIAL OR NO KNOWN CRYSTAL STRUCTURE (.pdf) Geert Vanhoyland, Bruker AXS GmbH, Karlsruhe, Germany
Afternoon New Frontiers in XRD in Pharmaceutical R&D
Session Co-chairs: Dr. Cyrus Crowder,
ICDD, Newtown Square, PA, U.S.A., and Dr. Harry Brittain, Center for Pharmaceutical Physics, Milford, NJ, U.S.A.
Invited PROTEIN POWDER DIFFRACTION AT THE ESRF (.pdf) Jonathan Wright, ESRF, Grenoble cedex, France
Contributed NEW POSSIBILITIES FOR X-RAY DIFFRACTOMETRY (.pdf) Bernd Hasse, Incoatec GmbH, Geesthacht, Germany
  Complementary Techniques
Session Chair: Dr. Raj Suryanarayanan
, University of Minnesota, Minneapolis, MN, U.S.A.
Invited ENVIRONMENTAL ATOMIC FORCE AND CONFOCAL RAMAN MICROSCOPIES IN PHARMACEUTICAL SCIENCE (.pdf) Greg Haugstad, University of Minnesota, Minneapolis, MN, U.S.A.
Contributed APPLICATION OF X-RAY SPECTROMETRY AT X-RAY ABSORPTION EDGES FOR INVESTIGATION OF HUMAN ALBUMIN (.pdf) Konstantin Pogrebitsky, Ioffe Physical-Technical Institute, Saint-Petersburg, Russia


Thursday, 7 May - 8.30 – 12.00
Round Robin Results from PPXRD-7
Session Chair: Dr. Fangling Needham
, ICDD, Newtown Square, PA, U.S.A.
Title of Paper Speaker & Affiliation

ROUND ROBIN for PHARMACEUTICAL COMPOUNDS (.pdf)

ROUND ROBIN for PHARMACEUTICAL COMPOUNDS - RESULTS ANALYSIS AND CLUSTER ANALYSIS (.pdf)

Fangling Needham, Cyrus Crowder, Timothy Fawcett, ICDD, Newtown Square, PA, U.S.A.

 

 

 

 

 

 

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