icdd Institute of Physics Chinese

PPXRD-12 Program - 20-24 May 2013 - Presenter Guidelines

  Chinese Program
Program in Chinese - PPXRD-12会议日程
   

(2 Day Workshop - 3 Days of Special Sessions - Poster Session)


TWO DAY WORKSHOP, 20-21 May 2013

Workshop will be in Chinese
讲习班将在物理所D栋D212房间举行。咖啡和展示设在会议室旁的走廊。午餐在物理所院子里的Wuke餐厅的四楼。
Workshop will be held at the Institute of Physics, Building D, Room D212. Coffee breaks will be held in the foyer near
the meeting room. Lunch will be served on the 4th floor of the Wuke restaurant, in the yard of the Institute of Physics.

 

WORKSHOP AGENDA Day 1- Monday, 20 May 2013
Workshop 08.30–17.30 | Break 10.15-10.30  | Lunch 12.00-13.00 | Break 15.00-15.15

Fundamentals of Pharmaceutical Powder X-ray Diffraction
Organizer & Instructors:
Dr. Shawn Yin, Bristol-Myers Squibb Company, New Brunswick, NJ, USA, shawn.yin@bms.com
Dr. Xiaolong Chen, Institute of Physics, Chinese Academy of Sciences, Beijing, China, xlchen@aphy.iphy.ac.cn
Dr. Alex Chen, Crystal Pharmatech, Suzhou, China, alex_chen@crystalpharmatech.com
Dr. Baoping Bob He, Bruker AXS, Inc., Madison, WI, USA, bhe@bruker.com

08.30-08.45

Workshop Opening Remarks

Dr. Shawn Yin

08.45-09.00

Submitting Your Difficult Problems

Dr. Shawn Yin

09.00-10.15

Basics of Powder & Single Crystal X-ray Diffraction

Dr. Xiaolong Chen

10.15-10.30

Break

10.30-11.00

PXRD Sample Preparation

Dr. Xiaolong Chen

11.00-12.00

PXRD Instruments

Dr. Baoping Bob He

12.00-13.00

Lunch

13.00-14.00

Instrument and Experiment Parameters

Dr. Baoping Bob He

14.00-15.00

Advanced PXRD Techniques

Dr. Baoping Bob He

15.00-15.15

Break

15.15-16.15

Special PXRD Instruments/Techniques/Devices for Pharmaceutical Science

Dr. Baoping Bob He

16.15-17.00

PXRD Data Interpretation

Dr. Xiaolong Chen

17.00-17.30

Question & Answer

All instructors

WORKSHOP AGENDA Day 2- Tuesday, 21 May 2013
Workshop 08.30–17.30 | Break 10.00-10.15  | Lunch 12.00-13.00 | Break 14.30-14.45

Applications of Pharmaceutical Powder X-ray Diffraction
Organizer & Instructors:
Dr. Shawn Yin, Bristol-Myers Squibb Company, New Brunswick, NJ, USA
Dr. Xiaolong Chen, Institute of Physics, Chinese Academy of Sciences, Beijing, China, xlchen@aphy.iphy.ac.cn
Dr. Alex Chen, Crystal Pharmatech, Suzhou, China, alex_chen@crystalpharmatech.com
Dr. Baoping Bob He, Bruker AXS, Inc., Madison, WI, USA, bhe@bruker.com

08.30-9.00

Pharmaceutical Industry Overview

Dr. Shawn Yin

09.00-10.00

Pharmaceutical Materials

Dr. Shawn Yin

10.00-10.15

Break

10.15-10.45

Pharmaceutical Solid State Hot Issues

Dr. Shawn Yin

10.45-12.00

Characterizing Pharmaceutical Materials

Dr. Shawn Yin

12.00-13.00

Lunch

13.00-14.00

PXRD for Qualitative and Quantitative Form Analysis

Dr. Alex Chen

14.00-14.30

Using Simulated PXRD Patterns

Dr. Alex Chen

14.30-14.45

Break

14.45-15.45

PXRD for Form Conversion Studies, Thermodynamics and Kinetics

Dr. Alex Chen

15.45-16.15

PXRD Experiments Under Non-ambient Conditions

Dr. Alex Chen

16.15-16.45

Drug Product Case Studies

Dr. Alex Chen

16.45-17.30

Attendee Problem Solving / Questions & Answers

All instructors

 


SPECIAL SESSIONS, 22-24 May 2013

Subject to change depending upon abstract submissions
Presentations will be given in English

* indicates presenter

专题会议将在物理所D栋D212房间举行。咖啡和展示设在会议室旁的走廊。午餐在物理所院子里的Wuke餐厅的四楼。
Sessions will be held at the Institute of Physics, Building D, Room D212. Coffee breaks and exhibits will be held in the foyer
near the meeting room. Lunch will be served on the 4th floor of the Wuke restaurant, in the yard of the Institute of Physics.

Wednesday, 22 May 2013 am Symposium

08.30-08.45

Welcoming Remarks & Introductions from the Program Chair
Dr. Cyrus Crowder, International Centre for Diffraction Data, Newtown Square, PA, USA

Qualitative and Quantitative Analysis
Chair: Dr. Detlef Beckers, PANalytical, Almelo, The Netherlands, detlef.beckers@panalytical.com

 

08.45-08.50

Introduction from the Chair

P26

08.50-09.35

Invited - X-ray Diffraction in Pharma Industry

K. Vyas, Dr. Reddy's Laboratories, Hyderabad, India

P20

09.35-10.05

Improving the Pharmaceutical Subfile for the ICDD PDF-4/Organics Database

C.E. Crowder*, S. Pagola, T.G. Fawcett, ICDD, Newtown Square, PA, USA
M. Suchomel, L. Ribaud, B. Toby, APS, Argonne National Laboratory, Argonne, IL, USA
J.A. Kaduk, Illinois Institute of Technology, Chicago, IL, USA

 

10.05-10.25

Break

 

P21

10.25-10.55

Effective Absorption Broadening of the Powder X-ray Diffraction and its Demonstration

K. Liu, Shanghai Institute of Technology, Shanghai, China

P23

10.55-11.25

Formulation Analysis with XRPD - Quality Control and Fake Drug Detection

U. Tiwari, PANalytical, Singapore
D. Beckers, PANalytical B.V., Almelo, The Netherlands

Wednesday, 22 May 2013 pm Symposium

New Frontiers in X-ray Diffraction in Pharmaceutical Research and Development
Chairs: Dr. Timothy Fawcett, International Centre for Diffraction Data, Newtown Square, PA, USA, fawcett@icdd.com
Dr. Xiaolong Chen, Institute of Physics, Chinese Academy of Sciences, Beijing, China, xlchen@aphy.iphy.ac.cn

 

13.00-13.05

Introduction from the Chair

P17

13.05-13.50

Invited - Hard X-ray Free Electron Lasers for Structural Biology: Structure Determination of Nano-crystals and Single Particles

Y.H. Dong, Beijing Synchrotron Radiation Facility, Institute of High Energy Physics, Chinese Academy of Sciences, Beijing, China

P11

13.50-14.35

Invited - Crystal Structure Analysis of Pharmaceuticals with Electron Diffraction

S. Nicolopoulos*, Nanomegas, Brussels, Belgium
M. Gemmi, IIT Researcher, Pisa, Italy
F. Gozzo, Excelsus Structural Solutions SPRL, Brussels, Belgium

 

14.35-14.55

Break

 

P13

14.55-15.25

Advances in Synchrotron XRPD for the Enhanced Characterization of Pharmaceuticals

F. Gozzo*, Excelsus Structural Solutions SPRL, Brussels, Belgium
I. Madsen, CSIRO Process Science and Engineering, Victoria, Australia
B. Aresta, C. Giannini, National Research Council, Institute of Crystallography, Bari, Italy

P19

15.25-15.55

Ultrafast X-ray Scattering and Spectroscopy: New Opportunities with Hard X-ray Free Electron Laser

M. Li, Institute of Physics, Chinese Academy of Sciences, Beijing, China

P31

15.55-16.25

Recent Advances in PPXRD Instrumentation and Application

B. He, Bruker AXS, Inc., Madison, WI, USA

 

POSTER SESSION, Wednesday, 22 May 2013

An evening cocktail hour and poster session of submitted papers will be held in the exhibit area.

The size of the poster board for PPXRD-12 is 90 cm wide x 120 cm high; 35 inches x 47 inches.
Poster authors can use push pins or tape to affix information to the poster board.

 

Thursday, 23 May 2013 am Symposium

Amorphous, Activated and Nanomaterials
Chair: Dr. Raj Suryanarayanan, University of Minnesota, Minneapolis, MN, USA, surya001@tc.umn.edu
Co-chair: Dr. Cyrus Crowder, International Centre for Diffraction Data, Newtown Square, PA, USA

 

08.30-08.35

Introduction from the Chair

P15

08.35-09.20

Invited - An Investigation of Non-Crystalline Materials Using X-ray Powder Diffraction

S. Bates, Triclinic Labs, West Layfayette, IN, USA

P33

09.20-10.05

Invited - Crystallization of Amorphous Phases - Characteriztization by Dielectric Spectroscopy and X-ray Diffractometry

R. Suryanarayanan, University of Minnesota, College of Pharmacy, Minneapolis, MN, USA

 

10.05-10.25

Break

 

P29

10.25-10.55

The Development of Nanomaterials and Amorphous References and their Use in Pharmaceutical Identification and Characterization

T.G. Fawcett, S.N. Kabekkodu, S.D. Gates, A.M. Gindhart, J.R. Blanton, C.E. Crowder, ICDD, Newtown Square, PA, USA

P30

10.55-11.25

The Determination of Amorphous Content

A. Kern, Bruker AXS, Inc., Karlsruhe, Germany

Non-Ambient Powder X-ray Diffraction
Chair: Dr. Hideo Toraya, Rigaku Corporation, Tokyo, Japan, toraya@rigaku.co.jp

 

13.00-13.05

Introduction from the Chair

P6

13.05-13.50

Invited - Application of Simultaneous XRD-DSC Methods for the Physical Characterization of Solid Pharmaceuticals

K. Terada, Toho University, Chiba, Japan

P22

13.50-14.20

Temperature Controlled Humidity Study of Trehalose Using X-ray Powder Diffraction

D. Beckers*, H. van Weeren, C.A. Reiss, O. Narygina, PANalytical B.V., Almelo, The Netherlands
U. Tiwari, PANalytical, Singapore
C. Resch, Anton Paar GmbH, Graz, Austria

P27

14.20-14.50

Phase Transition Behavior and High Temperature Crystal Structure Determination of Acyclovir

B. Yue, T. Konya, A. Kishi, Rigaku Corporation, Tokyo, Japan
E. Yonemochi, K. Terada, Toho University, School of Pharmaceutical Sciences, Funabashi, Chiba, Japan

 

14.50-15.10

Break

 

Thursday, 23 May 2013 pm Symposium

XRPD Techniques/Rietveld Refinement
Chair: Dr. Arnt Kern, Bruker AXS GmbH, Karlsruhe, Germany, arnt.kern@bruker.de

 

15.10-15.15

Introduction from the Chair

P8

15.15-15.45

Hydration / Dehydration Mechanism of Pharmaceutical Crystals Revealed by SDPD Method

H. Uekusa*, K. Fujii, Tokyo Institute of Technology, Japan

P12

15.45-16.15

Method Validation of X-ray SDPD Related to the Organic and Pharmaceutical Crystals

W. Xiaoqing, P. Qingqing, C. Qiang*, L. Hui, School of Chemical Engineering, Sichuan University, Chengdu, China

P7

16.15-16.45

Dehydration / Hydration Processes of Quinolone Antibacterial Agent Crystals by Ab Initio Powder X-ray Structure Determination

A. Sakon*, H. Uekusa, Tokyo Institute of Technology, Tokyo, Japan

P9

16.45-17:15

Crystal Structure Determination and Rietveld Refinement of Two Anhydrous Rifampicin Polymorphs using High-Resolution Synchrotron X-ray Powder Diffraction

R.C. Seiceira*, A. Pitaluga Jr, T.C. dos Santos, Institute of Drug Technology, Farmanguinhos, Fiocruz, Rio de Janeiro, Brazil
A.L. Ibiapino, A.C. Trindade, F.F. Ferreira, Federal University of ABC, Natural and Human Sciences Center, Santo André, Brazil

Friday, 24 May 2013 am Symposium

Formulation & Product Development
Chair: Dr. Shawn Yin, Bristol-Myers Squibb Company, New Brunswick, NJ, USA, shawn.yin@bms.com

 

08.30-08.35

Introduction from the Chair

P32

08.35-09.20

Invited - Applications of XRD in Preformulation and Formulation Studies

R. Suryanarayanan, University of Minnesota, College of Pharmacy, Minneapolis, MN, USA

P18

09.20-10.05

Invited - Process-Induced Phase Changes and Potential Impacts on Drug Product Performance

D. Zhou, AbbVie, North Chicago, IL, USA

P4

10.05-10.35

Best Practices in Formulation Analyses by X-ray Diffraction

T.G. Fawcett*, S.N. Kabekkodu, S.D. Gates, A.M. Gindhart, J.R. Blanton, C.E. Crowder, International Centre for Diffraction Data, Newtown Square, PA, USA

 

10.35-10.55

Break

 

Polymorph, Salt & Co-crystal Screening
Chair: Dr. Alex Chen, Crystal Pharmatech, Suzhou, China, alex_chen@crystalpharmatech.com

 

10.55-11.00

Introduction from the Chair

P28

11.00-11.45

Invited - Smart Screening Practices Applied to Early Pharmaceutical Development

X. Zhang*, J. Wang, L. Zhang, Y. Zhang, R. Wenslow, A. Chen, Crystal Pharmatech, Suzhou, Jiangsu, China

P10

11.45-12.15

Mechanochemically Initiated Isoniazid–Benzoic Acid Cocrystal Formation Under Accelerated Conditions

I. Sarcevica, L. Orola, University of Latvia, Riga, Latvia
S. Belyakov, Latvian Institute of Organic Synthesis, Riga, Latvia

 

12.15-12.30

Group Discussion/Closing Remarks